Solid state NMR: new tools for insight into enzyme function.

PubWeight™: 1.12‹?› | Rank: Top 10%

🔗 View Article (PMID 17964133)

Published in Curr Opin Struct Biol on October 25, 2007

Authors

Ann McDermott1, Tatyana Polenova

Author Affiliations

1: Columbia University, Department of Chemistry, New York, NY 10027, United States. aem5@columbia.edu

Articles citing this

Dynamics of reassembled thioredoxin studied by magic angle spinning NMR: snapshots from different time scales. J Am Chem Soc (2009) 1.32

1H-13C/1H-15N heteronuclear dipolar recoupling by R-symmetry sequences under fast magic angle spinning for dynamics analysis of biological and organic solids. J Am Chem Soc (2011) 1.14

Spin diffusion driven by R-symmetry sequences: applications to homonuclear correlation spectroscopy in MAS NMR of biological and organic solids. J Am Chem Soc (2011) 1.13

Mechanically, magnetically, and "rotationally aligned" membrane proteins in phospholipid bilayers give equivalent angular constraints for NMR structure determination. J Phys Chem B (2010) 1.09

Determination of relative tensor orientations by γ-encoded chemical shift anisotropy/heteronuclear dipolar coupling 3D NMR spectroscopy in biological solids. Phys Chem Chem Phys (2010) 1.05

Recoupling of chemical shift anisotropy by R-symmetry sequences in magic angle spinning NMR spectroscopy. J Chem Phys (2012) 1.00

Structure and function of G protein-coupled receptors using NMR spectroscopy. Prog Nucl Magn Reson Spectrosc (2010) 1.00

Probing ground and excited states of phospholamban in model and native lipid membranes by magic angle spinning NMR spectroscopy. Biochim Biophys Acta (2011) 0.98

Solid-state nuclear magnetic resonance studies delineate the role of the protein in activation of both aromatic rings of thiamin. J Am Chem Soc (2011) 0.96

3D DUMAS: simultaneous acquisition of three-dimensional magic angle spinning solid-state NMR experiments of proteins. J Magn Reson (2012) 0.93

Broadband homonuclear correlation spectroscopy driven by combined R2(n)(v) sequences under fast magic angle spinning for NMR structural analysis of organic and biological solids. J Magn Reson (2013) 0.89

Accurate measurement of heteronuclear dipolar couplings by phase-alternating R-symmetry (PARS) sequences in magic angle spinning NMR spectroscopy. J Chem Phys (2014) 0.86

Retinal dynamics during light activation of rhodopsin revealed by solid-state NMR spectroscopy. Biochim Biophys Acta (2009) 0.85

Structure of the disulfide bond generating membrane protein DsbB in the lipid bilayer. J Mol Biol (2013) 0.83

Glassy dynamics of protein methyl groups revealed by deuteron NMR. J Phys Chem B (2013) 0.83

Targeted 13C-13C distance measurements in a microcrystalline protein via J-decoupled rotational resonance width measurements. Chemphyschem (2009) 0.82

Structural characterization of supramolecular assemblies by ¹³C spin dilution and 3D solid-state NMR. J Biomol NMR (2012) 0.81

NMR crystallography of enzyme active sites: probing chemically detailed, three-dimensional structure in tryptophan synthase. Acc Chem Res (2013) 0.79

Dynamics of Hydrophobic Core Phenylalanine Residues Probed by Solid-State Deuteron NMR. J Phys Chem B (2015) 0.79

Fast Motions of Key Methyl Groups in Amyloid-β Fibrils. Biophys J (2016) 0.77

Protonation states and catalysis: Molecular dynamics studies of intermediates in tryptophan synthase. Protein Sci (2015) 0.77

Switches of hydrogen bonds during ligand-protein association processes determine binding kinetics. J Mol Recognit (2014) 0.76

Multiple acquisitions via sequential transfer of orphan spin polarization (MAeSTOSO): How far can we push residual spin polarization in solid-state NMR? J Magn Reson (2016) 0.75

Comparative Dynamics of Methionine Side-Chain in FMOC-Methionine and in Amyloid Fibrils. Chem Phys Lett (2017) 0.75

Articles by these authors

Probing structure and dynamics of protein assemblies by magic angle spinning NMR spectroscopy. Acc Chem Res (2013) 1.58

Solid-state NMR studies of HIV-1 capsid protein assemblies. J Am Chem Soc (2010) 1.49

Dynamics of reassembled thioredoxin studied by magic angle spinning NMR: snapshots from different time scales. J Am Chem Soc (2009) 1.32

Motions on the millisecond time scale and multiple conformations of HIV-1 capsid protein: implications for structural polymorphism of CA assemblies. J Am Chem Soc (2012) 1.28

Enhanced sensitivity by nonuniform sampling enables multidimensional MAS NMR spectroscopy of protein assemblies. J Phys Chem B (2012) 1.22

Magic angle spinning solid-state NMR spectroscopy for structural studies of protein interfaces. resonance assignments of differentially enriched Escherichia coli thioredoxin reassembled by fragment complementation. J Am Chem Soc (2004) 1.21

Magic angle spinning NMR experiments for structural studies of differentially enriched protein interfaces and protein assemblies. J Am Chem Soc (2008) 1.17

Biochemical and structural characterization of the Pak1-LC8 interaction. J Biol Chem (2008) 1.17

Solid-state and solution NMR studies of the CAP-Gly domain of mammalian dynactin and its interaction with microtubules. J Am Chem Soc (2009) 1.14

1H-13C/1H-15N heteronuclear dipolar recoupling by R-symmetry sequences under fast magic angle spinning for dynamics analysis of biological and organic solids. J Am Chem Soc (2011) 1.14

Spin diffusion driven by R-symmetry sequences: applications to homonuclear correlation spectroscopy in MAS NMR of biological and organic solids. J Am Chem Soc (2011) 1.13

Resonance assignments and secondary structure analysis of E. coli thioredoxin by magic angle spinning solid-state NMR spectroscopy. J Phys Chem B (2005) 1.08

Determination of relative tensor orientations by γ-encoded chemical shift anisotropy/heteronuclear dipolar coupling 3D NMR spectroscopy in biological solids. Phys Chem Chem Phys (2010) 1.05

Multidimensional magic angle spinning NMR spectroscopy for site-resolved measurement of proton chemical shift anisotropy in biological solids. J Am Chem Soc (2013) 1.02

51V solid-state magic angle spinning NMR spectroscopy of vanadium chloroperoxidase. J Am Chem Soc (2006) 1.01

J-based 2D homonuclear and heteronuclear correlation in solid-state proteins. Magn Reson Chem (2007) 1.01

Recoupling of chemical shift anisotropy by R-symmetry sequences in magic angle spinning NMR spectroscopy. J Chem Phys (2012) 1.00

Magic angle spinning NMR reveals sequence-dependent structural plasticity, dynamics, and the spacer peptide 1 conformation in HIV-1 capsid protein assemblies. J Am Chem Soc (2013) 0.99

Backbone assignments in solid-state proteins using J-based 3D heteronuclear correlation spectroscopy. J Am Chem Soc (2007) 0.98

Disease-associated mutations in the p150(Glued) subunit destabilize the CAP-gly domain. Biochemistry (2010) 0.96

Solid-state nuclear magnetic resonance studies delineate the role of the protein in activation of both aromatic rings of thiamin. J Am Chem Soc (2011) 0.96

Resonance Assignments and Secondary Structure Analysis of Dynein Light Chain 8 by Magic Angle Spinning NMR Spectroscopy. Can J Chem (2011) 0.95

2H double quantum filtered (DQF) NMR spectroscopy of the nucleus pulposus tissues of the intervertebral disc. Magn Reson Med (2007) 0.95

51V solid-state magic angle spinning NMR spectroscopy and DFT studies of oxovanadium(V) complexes mimicking the active site of vanadium haloperoxidases. Inorg Chem (2003) 0.95

Dynein and dynactin leverage their bivalent character to form a high-affinity interaction. PLoS One (2013) 0.94

A time-saving strategy for MAS NMR spectroscopy by combining nonuniform sampling and paramagnetic relaxation assisted condensed data collection. J Phys Chem B (2012) 0.94

Magic angle spinning NMR spectroscopy of thioredoxin reassemblies. Magn Reson Chem (2007) 0.94

51V magic angle spinning NMR spectroscopy of Keggin anions [PVnW12-nO40](3+n)-: effect of countercation and vanadium substitution on fine structure constants. J Am Chem Soc (2004) 0.92

Solid-state NMR spectroscopy of protein complexes. Methods Mol Biol (2012) 0.91

Solid-state NMR and density functional theory studies of ionization states of thiamin. J Phys Chem B (2010) 0.90

Sensitivity gains, linearity, and spectral reproducibility in nonuniformly sampled multidimensional MAS NMR spectra of high dynamic range. J Biomol NMR (2014) 0.90

Broadband homonuclear correlation spectroscopy driven by combined R2(n)(v) sequences under fast magic angle spinning for NMR structural analysis of organic and biological solids. J Magn Reson (2013) 0.89

51V magic angle spinning NMR spectroscopy of six-coordinate Lindqvist oxoanions: a sensitive probe for the electronic environment in vanadium-containing polyoxometalates. Counterions dictate the 51V fine structure constants in polyoxometalate solids. J Am Chem Soc (2003) 0.87

Investigating the vanadium environments in hydroxylamido V(V) dipicolinate complexes using 51V NMR spectroscopy and density functional theory. Inorg Chem (2007) 0.85

A novel disulfide-rich protein motif from avian eggshell membranes. PLoS One (2011) 0.83

Probing local environments in paramagnetic europium-substituted Keggin solids by 31P magic angle spinning NMR spectroscopy. J Phys Chem B (2006) 0.83

Chloro-substituted dipicolinate vanadium complexes: synthesis, solution, solid-state, and insulin-enhancing properties. J Inorg Biochem (2008) 0.83

51V solid-state NMR and density functional theory studies of vanadium environments in V(V)O2 dipicolinic acid complexes. J Chem Phys (2008) 0.82

Three-dimensional structure of CAP-gly domain of mammalian dynactin determined by magic angle spinning NMR spectroscopy: conformational plasticity and interactions with end-binding protein EB1. J Mol Biol (2013) 0.82

Combined zero-quantum and spin-diffusion mixing for efficient homonuclear correlation spectroscopy under fast MAS: broadband recoupling and detection of long-range correlations. J Biomol NMR (2014) 0.81

Fast magic angle spinning NMR with heteronucleus detection for resonance assignments and structural characterization of fully protonated proteins. J Biomol NMR (2014) 0.81

23Na TQF NMR imaging for the study of spinal disc tissue. J Magn Reson (2008) 0.81

Optical spectra of a novel polyoxometalate occluded within modified MCM-41. J Phys Chem B (2005) 0.80

(31)P magic angle spinning NMR spectroscopy for probing local environments in paramagnetic europium-substituted wells-dawson polyoxotungstates. Inorg Chem (2007) 0.79

The application of 23Na double-quantum-filter (DQF) NMR spectroscopy for the study of spinal disc degeneration. Magn Reson Med (2008) 0.79

(51)V solid-state NMR and density functional theory studies of eight-coordinate non-oxo vanadium complexes: oxidized amavadin. Dalton Trans (2009) 0.78

Characterization of noninnocent metal complexes using solid-state NMR spectroscopy: o-dioxolene vanadium complexes. Inorg Chem (2011) 0.77

31P magic angle spinning NMR spectroscopy of paramagnetic rare-earth-substituted Keggin and Wells-Dawson solids. J Am Chem Soc (2007) 0.76

HIV-1 Capsid Function is Regulated by Dynamics: Quantitative Atomic-Resolution Insights by Integrating Magic-Angle-Spinning NMR, QM/MM, and MD. J Am Chem Soc (2016) 0.75

Protein NMR spectroscopy: spinning into focus. Nat Chem (2011) 0.75

Improving dipolar recoupling for site-specific structural and dynamics studies in biosolids NMR: windowed RN-symmetry sequences. Phys Chem Chem Phys (2016) 0.75

Internuclear (31)P-(51)V distance measurements in polyoxoanionic solids using rotational echo adiabatic passage double resonance NMR spectroscopy. J Am Chem Soc (2007) 0.75

Premicellar complexes of sphingomyelinase mediate enzyme exchange for the stationary phase turnover. Biochim Biophys Acta (2005) 0.75

NMR crystallography for structural characterization of oxovanadium(V) complexes: deriving coordination geometry and detecting weakly coordinated ligands at atomic resolution in the solid state. Inorg Chem (2015) 0.75

Correction: Analysis of local molecular motions of aromatic sidechains in proteins by 2D and 3D fast MAS NMR spectroscopy and quantum mechanical calculations. Phys Chem Chem Phys (2017) 0.75